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Tenth Tetrahedron Symposium

Tetrahedron

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Articles in Press

Volume 65 (2009)

Volume 65, Issue 7
pp. 1207-1524 (14 February 2009)

Volume 65, Issue 6
pp. 1079-1206 (7 February 2009)

Volume 65, Issue 5
pp. 941-1078 (31 January 2009)

Volume 65, Issue 4
pp. 699-940 (24 January 2009)

Volume 65, Issue 3
pp. 581-698 (17 January 2009)

Volume 65, Issue 2
pp. 427-580 (10 January 2009)

Volume 65, Issue 1 - selected
pp. 1-426 (3 January 2009)

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Volume 65, Issue 1, Pages 1-426 (3 January 2009)

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articles 1 - 58

1.

Editorial board
Page IFC
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2.

Graphical contents list
Pages 1-15
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Report

3.

An overview of stereoselective synthesis of α-aminophosphonic acids and derivatives
Pages 17-49
Mario Ordóñez, Haydée Rojas-Cabrera, Carlos Cativiela
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Graphical abstract

Articles

4.

Jaspamides M–P: new tryptophan modified jaspamide derivatives from the sponge Jaspis splendans
Pages 51-56
Fulvio Gala, Maria Valeria D'Auria, Simona De Marino, Valentina Sepe, Franco Zollo, Charles D. Smith, Staci N. Keller, Angela Zampella
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Graphical abstract

5.

Synthesis of 7-(E)-alkenyl-4-amino-3-quinolinecarbonitriles via Pd-mediated Heck, Stille, and Suzuki reactions
Pages 57-61
Yanong D. Wang, Minu Dutia, M. Brawner Floyd, Amar S. Prashad, Dan Berger, Melissa Lin
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Graphical abstract

6.

Synthesis and crystal structures of fluorescent receptors for 9-butyladenine
Pages 62-69
Bassam Lamale, William P. Henry, Lee M. Daniels, Cungen Zhang, Suzane M. Klein, Yu Lin Jiang
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Graphical abstract

7.

S-Methylidene agents: preparation of chiral non-racemic heterocycles
Pages 70-76
David C. Forbes, Sampada V. Bettigeri, Samit A. Patrawala, Susanna C. Pischek, Michael C. Standen
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Graphical abstract

8.

Carboxylic acid to thioamide hydrogen bonding
Pages 77-82
Suchitra Datta, David A. Lightner
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Graphical abstract
[6]-Semirubin (X=O) is an intramolecularly hydrogen-bonded monomer in non-polar solvents that is favored over the intermolecularly hydrogen-bonded dimer, with Kassoc 25,000. [6]-Thiosemirubin (X=S) is a dimer, with Kassoc 200.

9.

Organic base catalyzed carbonyl allylation of methyl trifluoropyruvate with activated alkenes
Pages 83-86
Fan Zhang, Xiao-Jin Wang, Chen-Xin Cai, Jin-Tao Liu
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Graphical abstract

10.

Highly selective complexation of metal ions by the self-tuning tetraazacalixpyridine macrocycles
Pages 87-92
Han-Yuan Gong, De-Xian Wang, Qi-Yu Zheng, Mei-Xiang Wang
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Graphical abstract

11.

A convenient approach toward the synthesis of enantiopure isomers of DMDP and ADMDP
Pages 93-100
En-Lun Tsou, Yao-Ting Yeh, Pi-Hui Liang, Wei-Chieh Cheng
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Graphical abstract

12.

Efficient one-pot synthesis of benzopyranobenzopyrans and naphthopyranobenzopyrans by domino aldol-type reaction/hetero Diels–Alder reaction of resorcinols and naphthols
Pages 101-108
Yong Rok Lee, Yun Mi Kim, Sung Hong Kim
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Graphical abstract

13.

Remarkably selective saccharide recognition by solid-supported peptide boronic acids
Pages 109-114
Peter J. Duggan, Daniel A. Offermann
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Graphical abstract

14.

A novel synthetic route for the total synthesis of (±)-uleine
Pages 115-118
Suleyman Patir, Nesimi Uludag
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15.

On the reaction of some 5-polyfluoroaryl-1,2,4-oxadiazoles with methylhydrazine: synthesis of fluorinated indazoles
Pages 119-127
Antonio Palumbo Piccionello, Andrea Pace, Paola Pierro, Ivana Pibiri, Silvestre Buscemi, Nicolò Vivona
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16.

Synthesis of non-proteinogenic amino acids using Michael addition to unsaturated orthopyroglutamate derivative
Pages 128-133
Makoto Oba, Tsuneki Saegusa, Naohiro Nishiyama, Kozaburo Nishiyama
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Graphical abstract

17.

Di-tert-butyl dicarbonate: a versatile carboxylating reagent
Pages 134-138
John Kallikat Augustine, Y. Arthoba Naik, Veeramani Vairaperumal, Sharmila Narasimhan
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Graphical abstract

18.

Inverse stereoselectivity in the nucleophilic attack on five-membered ring oxocarbenium ions. Application to the total synthesis of 7-epi-(+)-goniofufurone
Pages 139-144
Luís Hernández-García, Leticia Quintero, Herbert Höpfl, Martha Sosa, Fernando Sartillo-Piscil
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Graphical abstract

19.

Preparations of bis[2-(2-arylethynyl)-3-thienyl]arenes and bis[2-{2-(trimethylsilyl)ethynyl}-3-thienyl]arenes
Pages 145-151
Kozo Toyota, Kazuyuki Okada, Hiroshi Katsuta, Noboru Morita
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Graphical abstract

20.

Synthesis and thermal behavior of chiral oligomers derived from cholesterol
Pages 152-157
K.C. Majumdar, S. Chakravorty, N. Pal, Nandiraju V.S. Rao
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21.

Highly efficient Cu-catalyzed oxidative coupling of tertiary amines and siloxyfurans
Pages 158-163
Youming Shen, Ze Tan, De Chen, Xunbo Feng, Mo Li, Can-Cheng Guo, Chengliang Zhu
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Graphical abstract

22.

A class of 18(13→14)-abeo-schiartane skeleton nortriterpenoids from Schisandra propinqua var. propinqua
Pages 164-170
Chun Lei, Jian-Xin Pu, Sheng-Xiong Huang, Ji-Jun Chen, Jing-Ping Liu, Li-Bin Yang, Yun-Bao Ma, Wei-Lie Xiao, Xiao-Nian Li, Han-Dong Sun
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Graphical abstract

23.

Preparation of (1R,1′R)-1,1′-(anthracene-9,10-diyl)bis(2,2,2-trifluoroethanamine): a chiral diamine with low basicity
Pages 171-176
Carla Estivill, Julen Mendizabal, Albert Virgili, Eva Monteagudo, Teresa Flor, Francisco Sánchez-Ferrando, Angel Alvarez-Larena, Juan F. Piniella
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Graphical abstract

24.

Enantioselective synthesis of 11-substituted 2- or 3-methoxy-17-vinylgona-1,3,5(10)-trien-13-ols
Pages 177-193
Delphine Moraleda, Michel Giorgi, Maurice Santelli
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Graphical abstract

25.

The first synthesis of ent-agelasine F
Pages 194-199
Ágnes Proszenyák, Morten Brændvang, Colin Charnock, Lise-Lotte Gundersen
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Graphical abstract

26.

Microwave-assisted manganese(III) acetate based oxidative cyclizations of alkenes with β-ketosulfones
Pages 200-205
Christophe Curti, Maxime D. Crozet, Patrice Vanelle
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Graphical abstract

27.

Efficient microwave-assisted synthesis of 4-amino-2-benzazepin-3-ones as conformationally restricted dipeptide mimetics
Pages 206-211
Beatrice Severino, Ferdinando Fiorino, Antonella Esposito, Francesco Frecentese, Francesca De Angelis, Elisa Perissutti, Giuseppe Caliendo, Vincenzo Santagada
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Graphical abstract

28.

Formal total synthesis of (–)- and (+)-balanol: two complementary enantiodivergent routes from vinyloxiranes and vinylaziridines
Pages 212-220
Jacqueline Gilmet, Bradford Sullivan, Tomas Hudlicky
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Graphical abstract

29.

Endoplasmic reticulum (ER) stress protecting compounds from the mushroom Mycoleptodonoides aitchisonii
Pages 221-224
Jae-hoon Choi, Madoka Horikawa, Hiroshi Okumura, Shinya Kodani, Kaoru Nagai, Daisuke Hashizume, Hiroyuki Koshino, Hirokazu Kawagishi
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Graphical abstract

30.

Synthesis and stereochemical assignment of (+)-Cladospolide D
Pages 225-231
Ke-Jhen Lu, Chia-Hsiu Chen, Duen-Ren Hou
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Graphical abstract

31.

Density functional theory rationalization of the substituent effects in trifluoromethyl-pyridinol derivatives
Pages 232-239
Jorge A. Fallas, Leticia González, Inés Corral
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Graphical abstract
Trifluoromethyl-pyrinidol derivatives show unexpected geometrical arrangements and proton affinity (PA) scale.

32.

Design, synthesis and conformational analysis of turn inducer cyclopropane scaffolds: microwave assisted amidation of unactivated esters on catalytic solid support to obtain γ-turn mimic scaffolds
Pages 240-246
Surinderjit Singh Bhella, Munusamy Elango, Mohan Paul S. Ishar
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Graphical abstract

33.

Preparation and characterization of bis[4-dimethylamino-2-pyrimidyl] dichalcogenides (S, Se, Te): X-ray crystal structure of bis[4-dimethylamino-2-pyrimidyl] diselenide and its physicochemical behavior in microemulsion media
Pages 247-252
K.K. Bhasin, Ekta Arora, Khushwinder Kaur, Sung-Kyu Kang, Michael Gobel, T.M. Klapoetke, S.K. Mehta
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Graphical abstract
Bis[4-dimethylamino-2-pyrimidyl] dichalcogenides (S, Se, Te) compounds have been synthesized and characterized by various spectroscopic techniques. Molecular structure of bis[4-dimethylamino-2-pyrimidyl] diselenide has been established by single crystal X-ray analysis and its interactions in microemulsion media have also been established.

34.

Synthesis and antioxidant activity of [60]fullerene–flavonoid conjugates
Pages 253-262
Roger F. Enes, Andreia S.F. Farinha, Augusto C. Tomé, José A.S. Cavaleiro, Riccardo Amorati, Silvia Petrucci, Gian Franco Pedulli
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Graphical abstract

35.

Decarboxylative photosubstitution of dicyanobenzenes with aliphatic carboxylate ions
Pages 263-269
Tatsuya Itou, Yasuharu Yoshimi, Toshio Morita, Yuji Tokunaga, Minoru Hatanaka
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36.

Practical and versatile oxidation of alcohol using novel Na2WO4–H2O2 system under neutral conditions
Pages 270-274
Takemasa Hida, Hideo Nogusa
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Graphical abstract

37.

3D-structure of cycloreticulin C and glabrin A, cyclopeptides from the seeds of Annona reticulata
Pages 275-281
Alassane Wélé, Claudine Mayer, Dermigny Quentin, Yanjun Zhang, Alain Blond, Bernard Bodo
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38.

2,6-Bis(porphyrin)-substituted pyrazine: a new class of supramolecular synthon binding to a transition-metal ion and fullerene (C60)
Pages 282-288
Yusaku Eda, Kennosuke Itoh, Yoshio N. Ito, Toshio Kawato
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Graphical abstract

39.

Facile access to some chiral building blocks. Synthesis of verbalactone and exophilin A
Pages 289-299
Jian-Zhong Wu, Jian Gao, Guo-Bao Ren, Zhi-Bin Zhen, Yihua Zhang, Yikang Wu
Preview   PDF (526 K)
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Graphical abstract

40.

Synthesis, structure, and conformation of ortho-linked oxacalix[n]arene[n]hetarenes
Pages 300-304
Mingliang Ma, Hongxiu Wang, Xiaoyan Li, Longqing Liu, Haishan Jin, Ke Wen
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Graphical abstract

41.

Heterogeneous chiral Mn(III) salen catalysts for the epoxidation of unfunctionalized olefins immobilized on mesoporous materials with different pore sizes
Pages 305-311
Kai Yu, Zhicheng Gu, Runan Ji, Lan-Lan Lou, Shuangxi Liu
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Graphical abstract

42.

Laccase-catalyzed coupling of catharanthine and vindoline: an efficient approach to the bisindole alkaloid anhydrovinblastine
Pages 312-317
Francesca Sagui, Cosimo Chirivì, Gabriele Fontana, Silvia Nicotra, Daniele Passarella, Sergio Riva, Bruno Danieli
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Graphical abstract

43.

The synthesis of carbon linked bis-benzylisoquinolines using Mizoroki–Heck and Sonagashira coupling reactions
Pages 318-327
Uta Batenburg-Nguyen, Alison T. Ung, Stephen G. Pyne
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Graphical abstract

44.

N-(α-Amidoalkyl)benzotriazole-mediated synthesis of β′-amido β-diketones: a general synthetic protocol for N-[β-(3,5-di and 1,3,5-trisubstituted pyrazol-4-yl)alkyl] amides
Pages 328-335
İlhami Çelik, Nevin Kanışkan, Şule Kökten
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Graphical abstract

45.

A new route to thiopyran S,S-dioxide derivatives via an overall ring-enlargement protocol from 3-nitrothiophene
Pages 336-343
Lara Bianchi, Massimo Maccagno, Giovanni Petrillo, Egon Rizzato, Fernando Sancassan, Elda Severi, Domenico Spinelli, Marco Stenta, Andrea Galatini, Cinzia Tavani
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Graphical abstract

46.

Three-component one-pot synthetic route to 2-amino-5-alkylidene-thiazol-4-ones
Pages 344-350
Marko Anderluh, Marko Jukič, Rok Petrič
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Graphical abstract

47.

A new synthetic approach towards isoquinobenzazepinone and isoindolinobenzazepinone using acid-mediated cyclisation and Heck reaction
Pages 351-356
Wong Phakhodee, Poonsakdi Ploypradith, Poolsak Sahakitpichan, Somsak Ruchirawat
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Graphical abstract

48.

γ-Amino vinyl sulfoxides in asymmetric synthesis. Synthesis of optically pure α-substituted β-amino nitriles
Pages 357-363
Ricardo Alfaro, Francisco Yuste, Benjamín Ortiz, Rubén Sánchez-Obregón, José L. García Ruano
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Graphical abstract

49.

Task-specific ionic liquid as base, ligand and reaction medium for the palladium-catalyzed Heck reaction
Pages 364-368
Lei Wang, Hongji Li, Pinhua Li
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Graphical abstract

50.

Isolation of new carbamate- or pyridine-containing natural products, fuzanins A, B, C, and D from Kitasatospora sp. IFM10917
Pages 369-373
Wataru Aida, Takashi Ohtsuki, Xiaofan Li, Masami Ishibashi
Preview   PDF (204 K)
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Graphical abstract

51.

Calix[4]arene bisphosphite ligands bearing two distal 2,2′-biphenyldioxy or 2,2′-binaphthyldioxy moieties: conformational flexibility and allyl–palladium complexes
Pages 374-382
Arindam Sarkar, Setharampattu S. Krishnamurthy, Munirathinam Nethaji
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Graphical abstract
Conformational exchange of novel calix[4]arene bisphosphite ligands and its freezing by complexation are presented.

52.

Influence of an ortho-sulfinyl group on the configurational stability of α-lithiated aryloxiranes: deuteration of tolylsulfinyl styrene oxides
Pages 383-388
Vito Capriati, Saverio Florio, Renzo Luisi, Antonio Salomone, Maria Giovanna Tocco, Ana M. Martín Castro, José Luis García Ruano, Esther Torrente
Preview   PDF (325 K)
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Graphical abstract

53.

Alkylations of tricyclo[5.2.1.02,6]deca-4,8-dien-3-one by a cuprate reaction
Pages 389-395
Andries A. Volkers, Antonius J.H. Klunder, Binne Zwanenburg
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Graphical abstract

54.

Synthesis of γ-lactones by desymmetrization. A synthesis of (−)-muricatacin
Pages 396-399
M. Teresa Barros, M. Adilia Januario Charmier, Christopher D. Maycock, Thierry Michaud
Preview   PDF (211 K)
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Graphical abstract

55.

Synthesis of a polypseudorotaxane, polyrotaxane, and polycatenane using ‘click’ chemistry
Pages 400-407
Marc Bria, Julien Bigot, Graeme Cooke, Joël Lyskawa, Gouher Rabani, Vincent M. Rotello, Patrice Woisel
Preview   PDF (448 K)
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Graphical abstract

56.

Synthesis, IR and NMR characterization and ion extraction properties of tetranonylcalix[4]resorcinol bearing acetylhydrazone groups
Pages 408-417
Sergey N. Podyachev, Nadezda E. Burmakina, Viktor V. Syakaev, Svetlana N. Sudakova, Roald R. Shagidullin, Alexander I. Konovalov
Preview   PDF (565 K)
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Graphical abstract

57.

Studies on the Toxic Oil Syndrome: proposal of a mechanism for the thermal conversion of 3-N-phenylamino-1,2-propanediol esters into anilides under deodorisation conditions
Pages 418-426
Jordi Escabrós, Ramon Crehuet, Angel Messeguer
Preview   PDF (509 K)
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Graphical abstract

58.

Calendar
Page I
Preview   PDF (61 K)
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articles 1 - 58

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